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sample dissolution

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how should i dissolve unknown sample having antimony in it.

tried H2SO4/H2O2 combination but not working .a residue settles down.

Antimony is often associated with lead compounds and must be removed in lead smelting. Look for information online for the common compounds of Sb and how those are made soluble. Post your ideas here and I will have a look at them. This is homework right?

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