Spezialemic

Can't get this simple reaction to work...

Recommended Posts

I'm trying to do the reaction shown here, but when I perform it I simply get two spots after w/u with DCM/H2O which are masses 213 and 251 (both +/- 1). sans an NMR, what might these two products be and how could I prevent their formation? Any ideas? Thanks!

Screen Shot 2019-06-04 at 9.38.02 AM.png

Share this post


Link to post
Share on other sites

It’s hard to say with just m/z, especially without knowing where those numbers are coming from. Are you monitoring consumption of your triazole by TLC? How good / pure are your reagents? Are you doing everything very dry? 

Share this post


Link to post
Share on other sites

Create an account or sign in to comment

You need to be a member in order to leave a comment

Create an account

Sign up for a new account in our community. It's easy!

Register a new account

Sign in

Already have an account? Sign in here.

Sign In Now