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lisab

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  1. 1. Write the balanced equation for the NaBH4 reduction of camphor, showing all likely products. 2. Identify the products of this reaction as structural isomers, enantiomers, or diastereomers. 3. Determine the limiting reagent and calculate the theoretical yield of the product (borneol and/or isoborneol)
  2. Considering that both analytical methods should be accurate to within 1% for the major component, do the results of the two methods agree? Explain in two sentences or less. If they do not agree, give a plausible explanation. my GC results Fraction 1 = 92.7% EtOAc 7.29% 1-BuOH Fraction 2 = 58.6% EtOAc 41.4% 1-BuOH Fraction 3 = 3.76% EtOAc 96.2% 1-BuOH RI results Fraction 1 = 87.5% EtOAc 12.5% 1-BuOH Fraction 2 = 49.5% EtOAc 50.5% 1-BuOH Fraction 3 = 2.5% EtOAc 97.5% 1-BuOH
  3. How would I know if my refractive index results agree with the shape of my plot of the distillate temperatures (vapor temp vs distillate volumes)? What do I need to look for?
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